HRID1910834

反应详情

EQUATION

反应方程式

HRID 1910834 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

1-(2-Cyclopent-1-enyl-2-oxo-ethyl)-2-methyl-pyridinium bromide salt (3.65 g, 12.94 mmol) was dissolved in methanol (25 mL) and hydrogenated over 10% palladium on carbon (180 mg). After completion of the reaction the Pd/C was removed by filtration through celite, washing twice with methanol. Concentration of the filtrate afforded 1-(2-cyclopentyl-2-oxo-ethyl)-2-methyl-pyridinium bromide salt (3.4 g, 93%).

WORKUP

后处理

  1. customwas removed by filtration through celite
  2. washwashing twice with methanol