HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanogen Bromide → HCID 24968262, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanogen Bromide | HCID 10476 | — |
| Reactant | HCID 68717082 | HCID 68717082 | — |
| Product | HCID 24968262 | HCID 24968262 | — |
Reaction Steps
In analogy to example 1b (S)-2-amino-4-(4-chloro-phenyl)-hexan-1-ol was reacted with cyanogen bromide to give (S)-4-[2-(4-chloro-phenyl)-butyl]-4,5-dihydro-oxazol-2-ylamine (mainly one epimer). Colourless oil. MS (ISP): 255.2 ([{37Cl}M+H]+), 253.2 ([{35Cl}M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08604061B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-8146b068860d4f63895f1bdbe54ad5ab |
| Source note | uspto-grants-2013_12 |