HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → 4-(3-(2,6-Dimethylbenzyloxy)phenyl)4-oxobutyric acid Potassium salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 9926783 | HCID 9926783 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-(3-(2,6-Dimethylbenzyloxy)phenyl)4-oxobutyric acid Potassium salt | HCID 20812328 | — |
Reaction Steps
The 4-(3-(2,6-Dimethylbenzyloxy)phenyl)-4-oxobutyric acid (Step D, 6.0 g, 19.4 mmol) was dissolved in abs ethanol (20 ml) by warming gently followed by addition of KOH (1.21 g) at 0° C. temperature. The reaction mixture was stirred for one hour, concentrated in vacuo and lyophilized to give the title compound as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08604083B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-3f2e52e312f34660ac383fd87c75f727 |
| Source note | uspto-grants-2013_12 |