HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1912041Generated: November 3, 2026
Hydroquinone → Ethyl 3-isobutyl-2-piperidin-1-ylcyclobutanecarboxylate
https://huagongshe.com/reaction/1912041
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydroquinone | HCID 785 | — |
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | 1-(4-Methyl-1-pentenyl)piperidine | HCID 86675030 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | Ethyl 3-isobutyl-2-piperidin-1-ylcyclobutanecarboxylate | HCID 71114720 | — |
Reaction Steps
1-(4-Methyl-1-pentenyl)piperidine (844 g) and acetonitrile (70 mL) were mixed. The ethyl acrylate (443 mL) and hydroquinone (447 mg) were added to the mixture. The resulting mixture was stirred at 95° C. overnight. The reaction mixture was concentrated in vacuo to give the title compound (994.08 g) as a crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08604069B2 |
|---|
| Source dataset | uspto-grants-2013_12 |
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| ORD ID | ord-5f2b1b1c37084f429c24b4bafa910bcc |
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| Source note | uspto-grants-2013_12 |
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