HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Methacrylate → HCID 86762181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Methacrylate | HCID 6658 | — |
| Reactant | Styrene | HCID 7501 | — |
| Reactant | 3-(Trimethoxysilyl)propyl methacrylate | HCID 17318 | — |
| Reactant | Pentanenitrile, 2,2'-(1,2-diazenediyl)bis[2-methyl- | HCID 206038 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 86762181 | HCID 86762181 | — |
Reaction Steps
Styrene (4.8 g), methyl methacrylate (2.85 g), 3-(trimethoxysilyl)propyl methacrylate (0.5 g) and 2,2′-azobis(2-cyanopentane) (0.3 g) are dissolved in 2-butanone (40 mL) and degassed using five vacuum/nitrogen purges. The reaction is refluxed for 24 hours and then precipitated into methanol (1 L), filtered, rinsed with additional methanol and sucked dry overnight. White polymer is obtained with Mw/Mn=10,400/7,200=1.45.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08609238B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-9a495fc0dd9f4dfa8ae6ab953742be48 |
| Source note | uspto-grants-2013_12 |