HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Methacrylate → HCID 169054, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Methacrylate | HCID 6658 | — |
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Glycidyl methacrylate | HCID 7837 | — |
| Reactant | Pentanenitrile, 2,2'-(1,2-diazenediyl)bis[2-methyl- | HCID 206038 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 169054 | HCID 169054 | — |
Reaction Steps
Styrene (4.8 g), methyl methacrylate (2.85 g), glycidyl methacrylate (0.3 g) and 2,2′-azobis(2-cyanopentane) (0.3 g) are dissolved in 2-butanone (40 mL) and degassed using five vacuum/nitrogen purges. The reaction is refluxed for 24 hours and then precipitated into methanol (1 L), filtered, rinsed with additional methanol and sucked dry overnight. A white polymer is obtained with Mw/Mn=16,000/8,300=1.9
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08609238B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-3b8bf3e9ef27406f999ed71847c32f0c |
| Source note | uspto-grants-2013_12 |