反应详情

The product from Example 105B and 1-adamantylacetyl chloride were processed using the method analogous to that described in Example 105C to afford the title compound. 1H NMR (300 MHz, DMSO-d6): δ ppm 1.45 (s, 9H), 1.59-1.67 (m, 12H), 1.95 (br s, 3H), 2.06 (s, 2H), 6.98 (dd, J=6.8, 4.1 Hz, 1H), 8.47 (dd, J=4.1, 1.7 Hz, 1H), 8.95 (dd, J=7.0, 1.9 Hz, 1H), 9.56 (s, 1H); MS (DCI) m/z 367 (M+H)+.