HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylprop-2-enoyl chloride → HCID 68749942, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylprop-2-enoyl chloride | HCID 66023 | — |
| Reactant | 3-Tert-butylpyrazolo[1,5-a]pyrimidin-2-amine | HCID 68755471 | — |
| Product | HCID 68749942 | HCID 68749942 | — |
Reaction Steps
The product from Example 105B and cinnamoyl chloride were processed using the method analogous to that described in Example 105C to afford the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 1.47 (s, 9H), 6.84 (d, J=14.9 Hz, 1H), 7.02 (dd, J=7.1, 4.1 Hz, 1H), 7.38-7.48 (m, 3H), 7.57-7.64 (m, 3H), 8.51 (dd, J=4.1, 1.7 Hz, 1H), 8.95 (dd, J=7.0, 1.9 Hz, 1H), 9.98 (s, 1H); MS (DCI) m/z 321 (M+H)+; EA calculated for C19H20N4O: C, 71.23; H, 6.29; N, 17.49. Found: C, 70.95; H, 6.06; N, 17.36.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08609669B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-a7173cfaaa7347dfab67a4a729cd10b6 |
| Source note | uspto-grants-2013_12 |