HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Chlorophenyl)acetic acid → HCID 68749933, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Chlorophenyl)acetic acid | HCID 15880 | — |
| Reactant | 3-Tert-butylpyrazolo[1,5-a]pyrimidin-2-amine | HCID 68755471 | — |
| Product | HCID 68749933 | HCID 68749933 | — |
Reaction Steps
The product from Example 105B and 4-chlorophenylacetic acid were processed using the method analogous to that described in Example 137 to afford the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 1.39 (s, 9H), 3.64 (s, 2H), 7.00 (dd, J=7.1, 4.0 Hz, 1H), 7.37-7.41 (m, 4H), 8.48 (dd, J=4.0, 1.6 Hz, 1H), 8.92 (dd, J=7.1, 1.6 Hz, 1H), 9.98 (s, 1H); MS (DCI) m/z 343 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08609669B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-38b7cee587884ab49d0286ac6e53ae93 |
| Source note | uspto-grants-2013_12 |