2-Cyclohexylvinyl boronic acid → HCID 86665184, compound

Participants

Reaction Steps

The product from Example 148A and 2-cyclohexylethenylboronic acid were processed using the method analogous to that described in Example 110C to provide the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 9.38 (s, 1H), 8.96 (dd, J=6.9, 1.7 Hz, 1H), 8.53 (dd, J=4.1, 1.7 Hz, 1H), 7.00 (dd, J=6.9, 4.0 Hz, 1H), 6.58 (dd, J=16.1, 6.8 Hz, 1H), 6.30 (dd, J=16.1, 1.2 Hz, 1H), 2.04-2.14 (m, 1H), 1.58-1.84 (m, 5H), 1.46 (s, 9H), 1.07-1.41 (m, 5H); MS (ESI) m/z 341 (M−H)−.

Provenance & Evidence