HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide diethylacetal → HCID 59186962, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide diethylacetal | HCID 70913 | — |
| Reactant | Ethyl 2-(5-bromopyridin-3-yl)acetate | HCID 54116619 | — |
| Product | HCID 59186962 | HCID 59186962 | — |
Reaction Steps
5.1 g (20.8 mmol) of the compound from Example 8A in 7.1 ml (6.2 g, 41.8 mmol) of dimethylformamide diethyl acetal are heated at 100° C. for 16 h. After cooling, the mixture is concentrated under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08609698B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-80e3d7f797304050959edbf9d9291729 |
| Source note | uspto-grants-2013_12 |