Sulfuryl chloride → HCID 19067137, compound

HRID 1913544Notes

Reaction equation

HRID 1913544 reaction equation
[C:1]([O:4][CH:5]([O:7][C:8](SCC)=[O:9])[CH3:6])(=[O:3])[CH3:2].S(Cl)([Cl:16])(=O)=O>>[C:1]([O:4][CH:5]([O:7][C:8]([Cl:16])=[O:9])[CH3:6])(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 24648Sulfuryl chlorideHCID 86210218HCID 86210218, compound

Product 1

HCID 19067137HCID 19067137, compound

Procedure

The compound (394 mg) obtained in Step 1 of this Example was cooled to −30° C. Sulfuryl chloride (175 μL) was added thereto, and the mixture was then stirred for 30 minutes. The solvent in the reaction solution was distilled off under reduced pressure to obtain a crude product of the title compound.

Workup

  1. customwas cooled to −30° C
  2. distillationThe solvent in the reaction solution was distilled off under reduced pressure

Sources & evidence

ORD record
ord-5478d9f241814fe187427e08f905e969
Source dataset
uspto-grants-2013_12
Patent number
US08609710B2

Reaction notes

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