Hydrazine → 4-Amino-3-chloro-5-fluoro-6-hydrazinopicolinonitrile

HRID 1913899Notes

Reaction equation

[NH2:1][C:2]1[C:7]([F:8])=[C:6](F)[N:5]=[C:4]([C:10]#[N:11])[C:3]=1[Cl:12].[NH2:13][NH2:14]>>[NH2:1][C:2]1[C:7]([F:8])=[C:6]([NH:13][NH2:14])[N:5]=[C:4]([C:10]#[N:11])[C:3]=1[Cl:12]

Participants

Reactant 2

HCID 9321Hydrazine

HCID 704973794-Amino-3-chloro-5,6-difluoropicolinonitrile

Product 1

HCID 704958804-Amino-3-chloro-5-fluoro-6-hydrazinopicolinonitrile

Procedure

reacting the fluoro substituent in the 6-position of 4-amino-3-chloro-5,6-difluoropicolinonitrile (Formula C) with hydrazine to produce 4-amino-3-chloro-5-fluoro-6-hydrazinopicolinonitrile (Formula D)

Sources & evidence

ORD record: ord-8d7a8547edfb4203a5058643124d8627
Source dataset: uspto-grants-2013_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08609853B2

Reaction notes

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