HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1914404Generated: October 29, 2026
Triethyl Phosphate → 9H-Carbazole, 2-methyl-
https://huagongshe.com/reaction/1914404
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethyl Phosphate | HCID 6535 | — |
| Reactant | 4'-Methyl-2-nitro-1,1'-biphenyl | HCID 10443194 | — |
| Product | 9H-Carbazole, 2-methyl- | HCID 19290 | 58.8% |
Reaction Steps
3 g of 2-(4-methylphenyl)nitrobenzene and 20 m of triethyl phosphate were heated and stirred at 160° C. for 6 hours. After triethyl phosphate was distilled off under reduced pressure, 10 ml of methanol was added, followed by filtration. The resulting solid was vacuum-dried to obtain 1.5 g of 2-methylcarbazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08610345B2 |
|---|
| Source dataset | uspto-grants-2013_12 |
|---|
| ORD ID | ord-b61ea94b4e404814a9c00ce4eea65c0f |
|---|
| Source note | uspto-grants-2013_12 |
|---|
