Triphenylsulfonium Bromide → HCID 131731096, compound

Participants

Reaction Steps

Tetrafluorodiglycolic acid disodium salt (0.45 g, 1.8 mmol) was dissolved in 6 mL of water and added slowly to a solution of triphenylsulfonium bromide (1.25 g, 3.6 mmol, dissolved in 12 mL dichloromethane). The mixture was stirred overnight at room temperature. The reaction mixture was evaporated to dryness (or to an oil stage) on a rotary evaporator. The product obtained from evaporation was washed with ethyl ether and dissolved using an excess amount of dichloromethane and filtered. After the evaporation of dichloromethane, the pure compound was obtained as a white solid.

Provenance & Evidence