HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1914982Generated: November 1, 2026
Methyl p-toluenesulfonate → HCID 22266844, compound
https://huagongshe.com/reaction/1914982
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl p-toluenesulfonate | HCID 6645 | — |
| Reactant | Thiazolo[4,5-b]pyridine, 2-(methylthio)- | HCID 11412747 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22266844 | HCID 22266844 | — |
Reaction Steps
To 0.626 g of 2-methylthiothiazolo[4,5-b]pyridine (Smith, et al. SULFUR LETTERS, 17, 197-216 (1994)) is added 0.71 g of methyl tosylate and the mixture is heated at 120° C. for one hour. After cooling to room temperature, 10 mL of ethyl acetate is added and the mixture is stirred for 30 minutes. The supernatant liquid is decanted and the product is recovered as an oily layer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08614302B2 |
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| Source dataset | uspto-grants-2013_12 |
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| ORD ID | ord-f5eb6e05ff484751981b88375f595dfd |
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| Source note | uspto-grants-2013_12 |
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