huagongshe.com
HRID1914996

反应详情

EQUATION

反应方程式

HRID 1914996 的结构方程式

REACTANTS

反应物

3
结构：ClP(Cl)(Cl)(Cl)Cl
HCID24819

Phosphorus pentachloride

Cl5P

结构：COc1ccc2c(c1)N(C)C(C)(C)CC2CS(=O)(=O)O
HCID12138186

未命名化合物

结构：CCN1c2cc(OC)ccc2C(CS(=O)(=O)O)=CC1(C)C
HCID12138189

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2c(c1)N(C)C(C)(C)CC2CS(=O)(=O)Cl
HCID12138193

未命名化合物

收率 78%

PROCEDURE

实验过程

(1-Methyl-7-methoxy-2,2-dimethyl-1,2,3,4-tetrahydroquinol-4-yl)-methane-sulfonic acid chloride (19) is prepared similarly to compound (16) using compound (3) and phosphorus pentachloride except that it is stirred for 18 hours at room temperature.