HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → 3-[4-(1-naphthyl)-phenyl]-9-phenyl-9H-carbazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 3-(4-Bromophenyl)-9-phenylcarbazole | HCID 51358293 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | 3-[4-(1-naphthyl)-phenyl]-9-phenyl-9H-carbazole | HCID 66684134 | — |
Reaction Steps
The Rf values of the objective substance and 3-(4-bromophenyl)-9-phenyl-9H-carbazole were respectively 0.57 and 0.65, which were obtained by silica gel thin layer chromatography (TLC) (with a developing solvent containing ethyl acetate and hexane in a 1:10 ratio).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08614334B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-b9d00294892e4b70860034facbecf5c2 |
| Source note | uspto-grants-2013_12 |