Hydrochloric Acid → HCID 178432373, compound

Participants

Reaction Steps

To 8.79 g 2-methyl-6-phenyl-5-(4-{[4-(5-pyridin-2-yl-1H-1,2,4-triazol-3-yl)piperidin-1-yl]methyl}phenyl)[1,2,4]triazolo[1,5-a]pyrimidine (prepared as described under example 37) in 88 ml methanol are added 2.85 ml hydrochloric acid solution (5.84N in methanol). The mixture is stirred at room temperature for 1 h. The solvent is removed to yield the desired product.

Provenance & Evidence