HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Ethylpyridin-2-amine → 6-Ethyl-5-iodopyridin-2-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Ethylpyridin-2-amine | HCID 89021 | — |
| Reactant | N-Iodosuccinimide | HCID 120273 | — |
| Product | 6-Ethyl-5-iodopyridin-2-amine | HCID 21663976 | — |
Reaction Steps
The title compound is synthesized according to general procedure GP1 starting from 10.0 g (83 mmol) 6-ethyl-pyridin-2-ylamine and 18.4 g (83 mmol) NIS. Yield after precipitation from the reaction mixture: 18.0 g (89%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618111B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-77d8b44ef4c1405d8399b0be82a3dcc6 |
| Source note | uspto-grants-2013_12 |