Sodium borohydride → HCID 58158143, compound

Participants

Reaction Steps

25 mg (0.043 mmol) of the compound from Example 3 were initially charged in 1 ml of THF and 0.1 ml of methanol, 0.8 mg (0.022 mmol) of sodium borohydride was added with stirring and the mixture was stirred at RT for 16 h. The reaction solution was diluted with about 2 ml of water and purified by preparative HPLC (Chromasil, water/acetonitrile+0.1% TFA).

Provenance & Evidence