HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 60659962, compound → HCID 62642302, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 60659962 | HCID 60659962 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 62642302 | HCID 62642302 | — |
Reaction Steps
100 mg Raney Nickel are added to a solution of 1.00 g (3.18 mmol) (4-bromo-2-nitro-phenyl)-(2-pyrrolidin-1-yl-ethyl)-amine in 100 mL MeOH. The reaction solution is stirred for 15 min at 3 bar H2 and RT. After filtration the solvent is eliminated i.vac. and the product is further reacted without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618132B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-7db26f7db2b44604b6788334eef24ed4 |
| Source note | uspto-grants-2013_12 |