HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Fluoro-2-methylbenzoyl chloride → 5-Fluoro-2-methyl-N-[2-methyl-4-(2-methyl-[1,3']bipyrrolidinyl-1'-yl)-phenyl]-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Fluoro-2-methylbenzoyl chloride | HCID 2737383 | — |
| Reactant | 2-Methyl-4-(2-methyl-[1,3']bipyrrolidinyl-1'-yl)-phenylamine | HCID 59401830 | — |
| Product | 5-Fluoro-2-methyl-N-[2-methyl-4-(2-methyl-[1,3']bipyrrolidinyl-1'-yl)-phenyl]-benzamide | HCID 59401876 | — |
Reaction Steps
The title compound was prepared in a manner substantially the same as Example 1 by coupling 2-methyl-4-(2-methyl-[1,3′]bipyrrolidinyl-1′-yl)-phenylamine with 5-fluoro-2-methyl-benzoyl chloride (from Alfa Aesar). LCMS: RT=1.56 minutes, MS: 396 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618159B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-139681c8ee8846b9b49a2da9a218392d |
| Source note | uspto-grants-2013_12 |