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4-Chlorobenzoyl chloride → 4-Chloro-N-[2-methyl-4-(2-(S)-methyl-[1,3'(S)]bipyrrolidinyl-1'-yl)-phenyl]-benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| 反応物 | 2-methyl-4-(2-(S)-methyl-[1,3'(S)]bipyrrolidinyl-1'-yl)-phenylamine | HCID 59401764 | — |
| 生成物 | 4-Chloro-N-[2-methyl-4-(2-(S)-methyl-[1,3'(S)]bipyrrolidinyl-1'-yl)-phenyl]-benzamide | HCID 59401881 | — |
反応手順
The title compound was prepared in a manner substantially the same as Example 1 by coupling 2-methyl-4-(2-(S)-methyl-[1,3′(S)]bipyrrolidinyl-1′-yl)-phenylamine with 4-chloro-benzoyl chloride. LCMS: RT=3.96 minutes, MS: 398 (M+H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08618159B2 |
| 出典データセット | uspto-grants-2013_12 |
| ORD ID | ord-c7d84c691374407a920fb4daf42ca1fe |
| 出典メモ | uspto-grants-2013_12 |