HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4'-Chlorobenzoyl)benzoic acid → HCID 58433818, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4'-Chlorobenzoyl)benzoic acid | HCID 66564 | — |
| Reactant | 4-Methoxybenzylamine | HCID 75452 | — |
| Product | HCID 58433818 | HCID 58433818 | 57% |
Reaction Steps
The named compound was synthesised from 2-(4-chlorobenzoyl)-benzoic acid (2.0 g, 7.6 mmol) and 4-methoxy benzylamine (0.542 mL, 4.18 mmol) using General Procedure B, purified by chromatography (Biotage SP4; 10-80% EtOAc/hexane) and obtained as a white solid (0.830 g, 57%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618158B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-0b83e27dffe74805aebd837b8175067b |
| Source note | uspto-grants-2013_12 |