4-Chloroaniline → HCID 86660691, compound

HRID 1917000Notes

Reaction equation

HRID 1917000 reaction equation
[C:1]12([CH:7]3[CH2:8][CH2:9][CH:4]1[CH:5]1[C:13](=[O:14])[O:12][C:10](=[O:11])[CH:6]13)[CH2:3][CH2:2]2.[Cl:15][C:16]1[CH:22]=[CH:21][C:19]([NH2:20])=[CH:18][CH:17]=1>C(Cl)(Cl)Cl>[Cl:15][C:16]1[CH:22]=[CH:21][C:19]([NH:20][C:10]([C@@H:6]2[C@H:7]3[C:1]4([CH2:3][CH2:2]4)[C@H:4]([CH2:9][CH2:8]3)[C@@H:5]2[C:13]([OH:12])=[O:14])=[O:11])=[CH:18][CH:17]=1

Participants

4

Reactant 2

HCID 78124-ChloroanilineHCID 585803091418115-02-2

Product 1

HCID 86660691HCID 86660691, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

Following General Procedure A, Compound 2 (0.042 g, 0.22 mmol) and 4-chloroaniline (0.028 g, 0.22 mmol) in chloroform (1.5 mL) were converted into the title compound, which was isolated as a white solid.

Sources & evidence

ORD record
ord-0ecda3c4ba0140ee95b72939153f2756
Source dataset
uspto-grants-2013_12
Patent number
US08618163B2

Reaction notes

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