Methanol → HCID 178442315, compound

HRID 1917446Notes

Reaction equation

HRID 1917446 reaction equation
[CH3:1][OH:2].[CH3:3][C:4]([C:8]1[N:12]=[CH:11][NH:10][C:9]=1[C:13]([OH:15])=O)([CH3:7])[CH:5]=[CH2:6].[CH:16](Cl)(Cl)Cl>>[CH2:1]([O:2][C:13]([C:9]1[NH:10][CH:11]=[N:12][C:8]=1[C:4]([CH3:7])([CH3:3])[CH:5]=[CH2:6])=[O:15])[CH3:16]

Participants

4

Reactant 3

HCID 887MethanolHCID 6212ChloroformHCID 178442314HCID 178442314, compound

Product 1

HCID 178442315HCID 178442315, compound

Procedure

Another byproduct isolated from a similar reaction (smaller scale) by further elution of the column with 5% MeOH/1% Et3N in chloroform was a compound suspected of being 5-(1,1-dimethyl-allyl)-3H-imidazole-4-carboxylic acid (0.27 g, 9%).

Sources & evidence

ORD record
ord-cc8266a498b249afa96db4b20380e4cb
Source dataset
uspto-grants-2013_12
Patent number
US08618292B2

Reaction notes

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