HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Hydroxyphthalimide → tert-Butyl (2-((1,3-dioxoisoindolin-2-yl)oxy)ethyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Hydroxyphthalimide | HCID 10665 | — |
| Reactant | tert-butyl N-(2-hydroxyethyl)carbamate | HCID 2733206 | — |
| Product | tert-Butyl (2-((1,3-dioxoisoindolin-2-yl)oxy)ethyl)carbamate | HCID 18929164 | — |
Reaction Steps
tert-Butyl 2-(1,3-dioxoisoindolin-2-yloxy)ethylcarbamate 2E was prepared with quantitative yield from tert-butyl 2-hydroxyethylcarbamate and N-hydroxyphthalimide by a procedure analogous to Example 2A, Step 1. ESI-MS: m/z 329.3 (M+Na)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618290B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-3440c10d5d5b450fbd0d75fdb898a70f |
| Source note | uspto-grants-2013_12 |