化工社化工社 化学情報印刷レポート · 研究参考用
Triphosgene → 6,6-Dimethyl-3-(6-(phenylethynyl)pyridazin-3-yl)-1,3-oxazinan-2-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triphosgene | HCID 94429 | — |
| 反応物 | 2-Methyl-4-(6-phenylethynyl-pyridazin-3-ylamino)-butan-2-ol | HCID 57516775 | — |
| 生成物 | 6,6-Dimethyl-3-(6-(phenylethynyl)pyridazin-3-yl)-1,3-oxazinan-2-one | HCID 53494699 | — |
反応手順
The title compound, a crystalline light yellow solid, MS: m/e=308.3 (M+H+), was prepared in accordance with the general method of Example 152, step 2 starting from 2-methyl-4-(6-phenylethynyl-pyridazin-3-ylamino)-butan-2-ol (Example 153, step 1) and triphosgene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08618296B2 |
| 出典データセット | uspto-grants-2013_12 |
| ORD ID | ord-5e25c063e8ee4a379ee0c8cbba22b476 |
| 出典メモ | uspto-grants-2013_12 |