Ammonia → HCID 66554144, compound

HRID 1918395Notes

Reaction equation

HRID 1918395 reaction equation
COCC1C=C([NH2:10])C=CC=1N.N.[N+:13]([C:16]1[CH:21]=[CH:20][C:19](Cl)=[CH:18][C:17]=1[CH2:23][O:24][CH3:25])([O-:15])=[O:14]>>[N+:13]([C:16]1[CH:21]=[CH:20][C:19]([NH2:10])=[CH:18][C:17]=1[CH2:23][O:24][CH3:25])([O-:15])=[O:14]

Participants

4

Reactant 3

HCID 222AmmoniaHCID 97938592-Methoxymethyl-p-phenylenediamineHCID 133378004-Chloro-2-(methoxymethyl)-1-nitrobenzene

Product 1

HCID 66554144HCID 66554144, compound

Procedure

Another embodiment of the present application relates to a method of making 2-methoxymethyl-1,4-benzenediamine comprising the steps: (a) introducing ammonia to a 4-nitro-3-methoxymethyl-chlorobenzene to obtain 4-nitro-3-methoxymethyl-aminobenzene; and (b) hydrogenating the 4-nitro-3-methoxymethyl-aminobenzene in the presence of a hydrogenation catalyst to obtain the 2-methoxymethyl-1,4-benzenediamine.

Sources & evidence

ORD record
ord-21ba7d0d1312428e909865aa58a582ce
Source dataset
uspto-grants-2013_12
Patent number
US08618326B2

Reaction notes

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