p-Chlorothiophenol → HCID 86617326, compound

Participants

Reaction Steps

N-methyl-N-phenyl-N′-phenylpropynamidine (0.23 g) was dissolved to chloroform (5 ml), chloroform (5 ml) solution of 4-chlorothiophenol (0.14 g) was added dropwise under ice-cooling and stirred for 14 hours at room temperature. The reaction solution was concentrated under reduced pressure. The residue was purified by silica gel column chromatography (hexane:ethyl acetate=7:1) to obtain N-methyl-N-phenyl-N′-phenyl-3-(4-chlorophenylthio)acrylamidine (0.22 g) as light yellow oil.

Provenance & Evidence