HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 86640675, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 86640674 | HCID 86640674 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86640675 | HCID 86640675 | — |
Reaction Steps
10 mmol 2-Acetylamino-4-cyanothiazole was dissolved in 10 ml anhydrous methanol, and 10 mmol sodium methoxide was added. Upon complete reaction of the starting materials, 20 mmol ammonium chloride was added, to carry out reaction in closed state for 12 hr. The reaction product was filtered to remove inorganic salt, and then the resultant filtrate was concentrated to obtain 2-acetylamino-4-thiazolformamidine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08168642B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-0d056e33c8a84dff883a0b00d08a8f63 |
| Source note | uspto-grants-2012_05 |