HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloroaniline → 4-chloro-N-(2,6-difluorobenzylidene)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloroaniline | HCID 7812 | — |
| Reactant | 2,6-Difluorobenzaldehyde | HCID 136284 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-chloro-N-(2,6-difluorobenzylidene)aniline | HCID 58149536 | — |
Reaction Steps
A mixture of 4-chloroaniline (1.84 g, 14.1 mmol) and 2,6-difluorobenzaldehyde 115 (1.55 mL, 14.1 mmol) in methanol (MeOH, 30 mL) was allowed to react for 18 hours at room temperature. The mixture was evaporated giving 4-chloro-N-(2,6-difluorobenzylidene)aniline 116 as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08168795B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-807eb14feed648d2978ead41869f01c5 |
| Source note | uspto-grants-2012_05 |