HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Diethoxymethyl)benzaldehyde → 1-[4-(diethoxymethyl)phenyl]-N-[(1-{[2-(trimethylsilyl)ethoxy]methyl}-1H-imidazol-2-yl)methyl]methanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Diethoxymethyl)benzaldehyde | HCID 595993 | — |
| Reactant | (1-((2-(trimethylsilyl)ethoxy)methyl)-1H-imidazol-2-yl)methanamine | HCID 21918674 | — |
| Product | 1-[4-(diethoxymethyl)phenyl]-N-[(1-{[2-(trimethylsilyl)ethoxy]methyl}-1H-imidazol-2-yl)methyl]methanamine | HCID 67164917 | — |
Reaction Steps
The same operation as in Example 2 was performed, except for using 4-(diethoxymethyl)benzaldehyde in place of 2-formyl-N,N-dimethyl-1H-imidazole-1-sulfonamide and 1-(1-{[2-(trimethylsilyl)ethoxy]methyl}-1H-imidazol-2-yl)methanamine in place of benzylamine, to obtain the title compound having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08168783B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-846c36c4376a48369ca972c569dc9890 |
| Source note | uspto-grants-2012_05 |