HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2E)-2-(hydroxymethylene)-4,4-dimethylcyclohexanone → (2E)-1-(4-chlorophenyl)-2-(hydroxymethylene)-4,4-dimethylcyclohexanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2E)-2-(hydroxymethylene)-4,4-dimethylcyclohexanone | HCID 12173050 | — |
| Reactant | HCID 178478191 | HCID 178478191 | — |
| Product | (2E)-1-(4-chlorophenyl)-2-(hydroxymethylene)-4,4-dimethylcyclohexanol | HCID 67079188 | — |
Reaction Steps
reacting the first protected (2E)-2-(hydroxymethylene)-4,4-dimethylcyclohexanone and 4-chlorophenyl magnesium bromide to provide the first protected (2E)-1-(4-chlorophenyl)-2-(hydroxymethylene)-4,4-dimethylcyclohexanol; and isolating or not isolating the first protected (2E)-1-(4-chlorophenyl)-2-(hydroxymethylene)-4,4-dimethylcyclohexanol; and
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08168784B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-226390f4579240b7a54defcb3a6c2571 |
| Source note | uspto-grants-2012_05 |