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HRID1920368

反应详情

EQUATION

反应方程式

HRID 1920368 的结构方程式

REACTANTS

反应物

2
结构：CCOC(OCC)C1CC(C)(C)CCC1=O
HCID58018341

未命名化合物

结构：Clc1ccc([Mg]Br)cc1
HCID178478191

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(OCC)C1CC(C)(C)CCC1(O)c1ccc(Cl)cc1
HCID58018339

未命名化合物

PROCEDURE

实验过程

reacting the 2-(diethoxymethyl)-4,4-dimethylcyclohexanone and 4-chlorophenyl magnesium bromide at about −60° C. to −10° C. to provide 1-(4-chlorophenyl)-2-(diethoxymethyl)-4,4-dimethylcyclohexanol and isolating or not isolating the 1-(4-chlorophenyl)-2-(diethoxymethyl)-4,4-dimethylcyclohexanol; and

WORKUP

后处理

  1. customat about −60° C. to −10° C.