HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde, 4-(2-methylpropyl)- → 3-(4-(2-Methylpropyl)phenyl)propanal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde, 4-(2-methylpropyl)- | HCID 577537 | — |
| Reactant | HCID 67159299 | HCID 67159299 | — |
| Product | 3-(4-(2-Methylpropyl)phenyl)propanal | HCID 15606649 | — |
Reaction Steps
4-Isobutyl 1-(3-methoxy-2-propen-1-yl)benzene was similarly prepared as described in Examples I and II. First, 4-isobutyl benzaldehyde (600 g, commercially available from Mitsubishi Gas Chemical Company, Inc.) was used to obtain 3-(4-isobutyl-phenyl)-propionaldehyde (568 g) with a boiling point of 119° C. at a pressure of 5 mmHg. 3-(4-Isobutyl-phenyl)-propionaldehyde (345 g) was consequently used to provide 4-isobutyl 1-(3-methoxy-2-propen-1-yl)benzene (188 g) with a boiling point of 124° C. at a pressure of 4 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08168834B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-9a920d54fba740ba999168a6948e75e6 |
| Source note | uspto-grants-2012_05 |