3-Fluorophenol → HCID 67219858, compound

HRID 1921257Notes

Reaction equation

[CH:1]1([C:8](Cl)=[O:9])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[F:11][C:12]1[CH:13]=[C:14]([OH:18])[CH:15]=[CH:16][CH:17]=1.FC1C=C(OC)C=CC=1>>[CH:1]1([C:8]([C:17]2[CH:16]=[CH:15][C:14]([OH:18])=[CH:13][C:12]=2[F:11])=[O:9])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

Reactant 3

HCID 97433-Fluorophenol

HCID 99753-Fluoroanisole

HCID 12556870Cycloheptanecarbonyl chloride

Product 1

HCID 67219858HCID 67219858, compound

Procedure

Using the same procedure but replacing 1-adamantyl carbonyl chloride by cycloheptane carbonyl chloride and 3-fluorophenol by 3-fluoroanisole, the following compound was obtained:

Workup

customthe following compound was obtained

Sources & evidence

ORD record: ord-62198da2e816478da580aad9839a7555
Source dataset: uspto-grants-2012_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08173679B2

Reaction notes

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