HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 58808669, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 58808670 | HCID 58808670 | — |
| Product | HCID 58808669 | HCID 58808669 | — |
Reaction Steps
5′-Ethyl-2′-methyl-6′-oxo-1′,6′-dihydro-[2,3′]bipyridinyl-6-carbaldehyde prepared in accordance with PREPARATION 11 is reacted with pyrrolidine as described in Method A, Example 123 to give the title compound. MS: m/e=298 (M+H). 1H NMR (CDCl3, δ ppm): 7.89 (t, 1H, J=7.8 Hz); 7.77 (s, 1H); 7.61 (d, 1H, J=7.8 Hz); 7.41 (d, 1H, J=7.8 Hz); 4.43 (s, 2H); 3.80 (m, 2H); 3.07 (m, 2H); 2.66 (q, 2H, J=7.4 Hz); 2.55 (s, 3H); 2.13 (m, 4H); 1.25 (t, 3H, J=7.4 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173682B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-0bca4c3d87944b5c8eed60962668c2e2 |
| Source note | uspto-grants-2012_05 |