2-Pyridinemethanamine → HCID 58808626, compound

Participants

Reaction Steps

Method 1, Example 205 is substantially repeated except for utilizing 5′-ethyl-2′-methyl-6′-oxo-1′,6′-dihydro-[2,3′]bipyridinyl-5-carboxylic acid and (pyridin-2-ylmethyl)-amine to afford the title compound. MS: m/e=349 (M+H). 1H NMR (δ ppm): 11.71 (s, 1H); 9.28 (t, 1H, J=5.8 Hz); 9.07 (s, 1H); 858 (s, 1H); 8.47 (dd, 1H, J=4.6 and 1.5 Hz); 8.24 (dd, 1H, J=8.3 and 2.5 Hz); 7.75 (m, 1H); 7.63 (d, 1H, J=8.3 Hz); 7.54 (s, 1H); 7.37 (dd, 1H, J=7.7 and 4.6 Hz); 4.53 (d, 2H, J=5.8 Hz); 2.42 (q, 2H, J=7.4 Hz); 2.35 (s, 3H); 1.11 (t, 3H, J=7.4 Hz).

Provenance & Evidence