HCID 20674654, compound → HCID 58808589, compound
Reaction equation
[CH2:1]([C:3]1[C:8](=[O:9])[NH:7][C:6]([CH3:10])=[C:5]([C:11]2[CH:12]=[N:13][CH:14]=[C:15]([C:17]([OH:19])=O)[CH:16]=2)[CH:4]=1)[CH3:2].[CH3:20][C:21]1[N:26]=[CH:25][C:24]([CH:27]([NH2:30])[CH2:28][CH3:29])=[CH:23][CH:22]=1>>[CH3:20][C:21]1[N:26]=[CH:25][C:24]([CH:27]([NH:30][C:17]([C:15]2[CH:16]=[C:11]([C:5]3[CH:4]=[C:3]([CH2:1][CH3:2])[C:8](=[O:9])[NH:7][C:6]=3[CH3:10])[CH:12]=[N:13][CH:14]=2)=[O:19])[CH2:28][CH3:29])=[CH:23][CH:22]=1Participants
3
Procedure
Method 1, Example 205 is substantially repeated except for utilizing 5′-ethyl-2′-methyl-6′-oxo-1′,6′-dihydro-[3,3′]bipyridinyl-5-carboxylic acid and 1-(6-methyl-pyridin-3-yl)-propyl amine to afford the title compound. MS: m/e=391 (M+H).
Sources & evidence
- ORD record
- ord-8fbe3f1de3ea483fb5282c80e9fc55b9
- Source dataset
- uspto-grants-2012_05
- Patent number
- US08173682B2
Reaction notes
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