N-Methylglycinamide → HCID 58808642, compound

HRID 1921503Notes

Reaction equation

HRID 1921503 reaction equation
[CH2:1]([C:3]1[C:8](=[O:9])[NH:7][C:6]([CH3:10])=[C:5]([C:11]2[CH:12]=[N:13][CH:14]=[C:15]([C:17]([OH:19])=O)[CH:16]=2)[CH:4]=1)[CH3:2].[CH3:20][NH:21][CH2:22][C:23]([NH2:25])=[O:24]>>[C:23]([CH2:22][N:21]([CH3:20])[C:17]([C:15]1[CH:16]=[C:11]([C:5]2[CH:4]=[C:3]([CH2:1][CH3:2])[C:8](=[O:9])[NH:7][C:6]=2[CH3:10])[CH:12]=[N:13][CH:14]=1)=[O:19])(=[O:24])[NH2:25]

Participants

3

Reactant 2

HCID 151411N-MethylglycinamideHCID 588087025'-Ethyl-2'-methyl-6'-oxo-1',6'-dihydro-[3,3']bipyridinyl-5-carboxylic acid

Product 1

HCID 58808642HCID 58808642, compound

Procedure

Method 1, Example 205 is substantially repeated except for utilizing 5′-ethyl-2′-methyl-6′-oxo-1′,6′-dihydro-[3,3′]bipyridinyl-5-carboxylic acid and 2-methylamino-acetamide to afford the title compound. MS: m/e=329 (M+H).

Sources & evidence

ORD record
ord-844d18fcd7cc462bb43fbb9b9c894b8a
Source dataset
uspto-grants-2012_05
Patent number
US08173682B2

Reaction notes

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