4-Pyridineethanamine → HCID 58808782, compound

Participants

Reaction Steps

Method 1, Example 205 is substantially repeated except for utilizing 5′-ethyl-2′-methyl-6′-oxo-1′,6′-dihydro-[3,3′]bipyridinyl-5-carboxylic acid and 2-(pyridin-4-yl)-ethyl-amine to afford the title compound. MS: m/e=363 (M+H). 1H NMR (δ ppm): 11.72 (s, 1H); 8.87 (d, 1H, J=2.1 Hz); 8.77 (t, 1H, J=5.4 Hz); 8.67 (d, 1H, 2.1 Hz); 8.47 (m, 2H); 8.04 (t, 1H, J=2.1 Hz); 7.29 (m, 3H); 3.57 (q, 2H, J=7.1 Hz); 2.89 (t, 2H, J=7.1 Hz); 2.42 (q, 2H, J=7.4 Hz); 2.17 (s, 3H); 1.11 (t, 3H, J=7.4 Hz).

Provenance & Evidence