HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(1H-Benzimidazol-2-yl)ethan-1-amine → 5'-Ethyl-2'-methyl-6'-oxo-1',6'-dihydro-[3,3']bipyridinyl-5-carboxylic acid [2-(1H-benzoimidazol-2-yl)-ethyl]-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(1H-Benzimidazol-2-yl)ethan-1-amine | HCID 415158 | — |
| Reactant | 5'-Ethyl-2'-methyl-6'-oxo-1',6'-dihydro-[3,3']bipyridinyl-5-carboxylic acid | HCID 58808702 | — |
| Product | 5'-Ethyl-2'-methyl-6'-oxo-1',6'-dihydro-[3,3']bipyridinyl-5-carboxylic acid [2-(1H-benzoimidazol-2-yl)-ethyl]-amide | HCID 58808778 | — |
Reaction Steps
Method 1, Example 205 is substantially repeated except for utilizing 5′-ethyl-2′-methyl-6′-oxo-1′,6′-dihydro-[3,3′]bipyridinyl-5-carboxylic acid and 2-(1H-benzoimidazol-2-yl)-ethyl-amine to afford the title compound. MS: m/e=402 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173682B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-33872874299348458b38ad8aed9281b7 |
| Source note | uspto-grants-2012_05 |