HCID 2724233, compound → HCID 69757016, compound

HRID 1921517Notes

Reaction equation

HRID 1921517 reaction equation
[CH2:1]([C:3]1[C:8](=[O:9])[NH:7][C:6]([CH3:10])=[C:5]([C:11]2[CH:12]=[N:13][CH:14]=[C:15]([C:17]([OH:19])=O)[CH:16]=2)[CH:4]=1)[CH3:2].[CH3:20][C:21]1[N:22]([CH2:29][CH2:30][NH2:31])[C:23]([N+:26]([O-:28])=[O:27])=[CH:24][N:25]=1>>[CH3:20][C:21]1[N:22]([CH2:29][CH2:30][NH:31][C:17]([C:15]2[CH:16]=[C:11]([C:5]3[CH:4]=[C:3]([CH2:1][CH3:2])[C:8](=[O:9])[NH:7][C:6]=3[CH3:10])[CH:12]=[N:13][CH:14]=2)=[O:19])[C:23]([N+:26]([O-:28])=[O:27])=[CH:24][N:25]=1

Participants

3

Reactant 2

HCID 2724233HCID 2724233, compoundHCID 588087025'-Ethyl-2'-methyl-6'-oxo-1',6'-dihydro-[3,3']bipyridinyl-5-carboxylic acid

Product 1

HCID 69757016HCID 69757016, compound

Procedure

Method 1, Example 205 is substantially repeated except for utilizing 5′-ethyl-2′-methyl-6′-oxo-1′,6′-dihydro-[3,3′]bipyridinyl-5-carboxylic acid and 2-(2-methyl-5-nitro-imidazol-1-yl)-ethyl-amine to afford the title compound. MS: m/e=411 (M+H).

Sources & evidence

ORD record
ord-223a94c7127f4828a7b544cbff1544cc
Source dataset
uspto-grants-2012_05
Patent number
US08173682B2

Reaction notes

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