HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4'-methoxyacetophenone → 5'-Ethyl-2'-methyl-6'-oxo-1',6'-dihydro-[3,3']bipyridinyl-5-carboxylic acid [2-(4-methoxy-phenyl)-2-oxo-ethyl]-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4'-methoxyacetophenone | HCID 412889 | — |
| Reactant | 5'-Ethyl-2'-methyl-6'-oxo-1',6'-dihydro-[3,3']bipyridinyl-5-carboxylic acid | HCID 58808702 | — |
| Product | 5'-Ethyl-2'-methyl-6'-oxo-1',6'-dihydro-[3,3']bipyridinyl-5-carboxylic acid [2-(4-methoxy-phenyl)-2-oxo-ethyl]-amide | HCID 58808520 | — |
Reaction Steps
Method 1, Example 205 is substantially repeated except for utilizing 5′-ethyl-2′-methyl-6′-oxo-1′,6′-dihydro-[3,3′]bipyridinyl-5-carboxylic acid and [2-(4-methoxy-phenyl)-2-oxo-ethyl]-amine to afford the title compound. MS: m/e=406 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173682B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-201d6b57df634de2ba5de3e4c716640f |
| Source note | uspto-grants-2012_05 |