HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Difluorobenzylamine → HCID 58808588, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Difluorobenzylamine | HCID 145211 | — |
| Reactant | 5-(5-Ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl)furan-2-carboxylic acid | HCID 67492417 | — |
| Product | HCID 58808588 | HCID 58808588 | 91% |
Reaction Steps
Method 1, Example 205 is substantially repeated except for utilizing 5-(5-ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl)furan-2-carboxylic acid and 3,5-difluoro-benzylamine to give the title compound (91% yield). LC/MS: RT 3.52 min; m/e 373 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173682B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-1f3ef87718884889b1c7e184ffdd1d94 |
| Source note | uspto-grants-2012_05 |