HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Trifluoromethyl)benzylamine → HCID 58808750, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Trifluoromethyl)benzylamine | HCID 76804 | — |
| Reactant | 5-(5-Ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl)furan-2-carboxylic acid | HCID 67492417 | — |
| Product | HCID 58808750 | HCID 58808750 | 60% |
Reaction Steps
Method 1, Example 205 is substantially repeated except for utilizing 5-(5-ethyl-2-methyl-6-oxo-1,6-dihydro-pyridin-3-yl)-furan-2-carboxylic acid and 4-trifluoromethyl-benzylamine to afford the title compound (60% yield). LC/MS: RT 2.95 min; m/e 405 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173682B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-318dddd7e8b64b49bc87636e0ec96b19 |
| Source note | uspto-grants-2012_05 |