Acetaldehyde → HCID 58808618, compound

HRID 1921548Notes

Reaction equation

[CH2:1]([C:3]1[C:4](=[O:15])[NH:5][C:6]([CH3:14])=[C:7]([C:9]2[O:10][CH:11]=[CH:12][CH:13]=2)[CH:8]=1)[CH3:2].[CH:16](=[O:18])[CH3:17]>>[CH2:1]([C:3]1[C:4](=[O:15])[NH:5][C:6]([CH3:14])=[C:7]([C:9]2[O:10][C:11]([CH:16]([OH:18])[CH3:17])=[CH:12][CH:13]=2)[CH:8]=1)[CH3:2]

Participants

Reactant 2

HCID 177Acetaldehyde

HCID 67492545HCID 67492545, compound

Product 1

HCID 58808618HCID 58808618, compound

Procedure

Example 267 is substantially repeated except for utilizing 3-ethyl-6-methyl-5-furan-2-yl-1H-pyridin-2-one prepared in accordance with the procedures of Example 44, Step 2 and acetaldehyde to afford the title compound. MS: m/e=248 (M+H).

Sources & evidence

ORD record: ord-6149cc8a4c4b41008d6490ed74bb198d
Source dataset: uspto-grants-2012_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08173682B2

Reaction notes

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