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HRID1921553

反应详情

EQUATION

反应方程式

HRID 1921553 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)Cl
HCID6367

Acetyl chloride

C2H3ClO

结构：CCc1cc(-c2ccc(CN)o2)c(C)[nH]c1=O
HCID58808718

5-[5-(Aminomethyl)-2-furanyl]-3-ethyl-6-methyl-2(1H)-pyridinone

C13H16N2O2

PRODUCTS

生成物

1
结构：CCc1cc(-c2ccc(CNC(C)=O)o2)c(C)[nH]c1=O
HCID58808654

未命名化合物

PROCEDURE

实验过程

Example 269 is substantially repeated except for utilizing 5-(5-aminomethylfuran-2-yl)-3-ethyl-6-methyl-1H-pyridin-2-one and acetyl chloride to afford the title compound. MS: m/e=275 (M+H). 1H NMR (D6-DMSO, δ ppm): 11.64 (s, 1H); 8.30 (t, 1H, J=5.3 Hz); 7.45 (s, 1H); 6.39 (d, 1H, J=3.2 Hz); 6.30 (d, 1H, J=3.2 Hz); 4.26 (d, 2H, J=5.3 Hz); 2.40 (q, 2H, J=7.4 Hz); 2.32 (s, 3H); 1.84 (s, 3H); 1.10 (t, 3H, J=7.4 Hz).